fig2

Photoinduced iron-catalyzed direct coupling of cycloalkanes and <i>N</i>-sulfonyl ketimines using air as oxidant

Figure 2. Scope of reaction. aReaction conditions: 1 (0.2 mmol), 2 (4.0 mmol), TBACl (2.0 equiv.) and FeCl3 (10 mol%) in 2.0 mL of DCM and irradiated under 6 W 385 nm LEDs at room temperature for 13 h under air atmosphere. b1 equiv. TFA was added. TBACl: Tetrabutylammonium chloride; DCM: dichloromethane; LEDs: light-emitting diodes; TFA: trifluoroacetic acid.

Chemical Synthesis
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